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Planetary ball milling nd2l

Jan 25, 2014 cles at the beginning of milling. A planetary ball mill (Torrey Hills- ND2L) with stainless steel cups (285 mL capacity) and balls (28 of 16 mm and 6 of 18 mm diameter) milled the powders in an argon (Ar) atmo-sphere. Ball to powder ratio was 30:1, and the mill speed was maintained at 200 RPM for durations of 0.25, 0.5, 1, 2, 4, 7, 11, and 19 hours

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